Fluid Loss Test
A fluid-loss test determines the relative effectiveness of a cement slurry to retain its water phase or to lose a portion of its water phase as a filtrate to the formation. Insufficient fluid loss control can result in the cement slurry dehydrating and bridging off the annulus, preventing the slurry from being pumped to its final location and leaving excess cement in the casing.
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Filter Cores for Dynamic HPHT® Filtration System
Fann engineers designed special filter cores for the Model 90 Dynamic HPHT Filtration System to conduct filter cake formation and permeability analysis.
The filter medium is a thick-walled cylinder with rock-like characteristics to simulate the build-up of filter cake on the formation. This provides more accurate filtration measurements. The entire internal length is subjected to pressurized fluid (sample). Filtrate flows through the core radially from the inside to the outside.
The filter medium is available in varying porosities and permeabilities to simulate down-hole formations.
Filter Cores are supplied in boxes of 10 cores of the same porosity.Ordering Information Part Number Porosity (Mean Pore Diameter) Permeability (Air) 210545 5 micron 750 milli-darcy 210546 10 micron 950 milli-darcy 210547 20 micron 2.8 darcy 213483 35 micron 5.5 darcy 210548 60 micron 6.7 darcy 210549 90 micron 13.5 darcy 210550 150 micron 26.5 darcy 210551 190 micron 75 darcy Ceramic Filter Core Specifications Nominal Core Dimensions Maximum Recommended Values Inside Diameter 1.014 +/- 0.005 Mud weight, lb/gal (sg) Rate, mL/min CDI Outside Diameter 1.510 +/- 0.020 9-12 (1.08-1.44) 0.22 25 Length 1.114 +/- 0.005 12-15 (1.44-1.80) 0.18 20 15 or greater (1.80 +) 0.14 16
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Filter Paper
This Filter paper is a calendared, hardened, qualitative low-ash filter paper used to filter fine precipitates with the following qualities:
- A very slow, extra dense paper made from 100% cotton linters
- Lint-free surface
- Highly resistant to acid and alkaline solutions.
Ordering Information Part No Description 206056 Filter paper 6.35 cm, 100 in box (for HPHT). 206051 Filter paper 9 cm, 100 in box (for LPLT). Specifications Basis Weight 92 (g / m2) Caliper 0.137 (mm) Densometer 172.3 (Gurley secs / 100 cc air 0.1 sq. in) Water absorbency 0.9 Klemm (1/16 inch / min.)
8.9 (g / 100 cm2)Wet Strength 75 psi Particle Retention
All paper grades are described by the type of particles retained, in accordance with ASTM Standard Methods. The particle size retention range for this paper is 2-5μm (microns). The filter paper meets or exceeds the standards established by the American Petroleum Institute as published in API Recommended Practice 13B-1 and API Recommended Practice 13B-2.
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Filter Press Cell Clamp
HPHT Filter Press Cells are commonly used to test drilling fluids under high-pressure and high-temperature conditions. During this testing the possibility exists that the test fluid may solidify and plug the entrance and exit valve stems to the cell. Laboratory technicians are increasingly concerned about opening a HPHT Filter Press cell with pressure trapped inside.
Fann has developed a bench top cell clamp to maintain force on the lid while the set screws are removed. Once the screws are removed, the lid can be allowed to slowly rise and release any trapped pressure in a controlled manner.
Two height clamps are available for the different cell sizes.Ordering Information Part No Description 232207 Clamp for 175ml HPHT Filter Press Cell 232208 Clamp for 500ml HPHT Filter Press Cell
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Filter Press HPHT 500 ML
500 ml HPHT Filter Press units can be pressurized to 1800 psig on the cell and 750 psig on the back pressure receiver. Maximum operating temperature is 500°F. For operation above 400°F, the filter paper should be backed with a glass fiber filter, or a stainless steel filter.
HPHT Filter Presses are available in various component configurations which allow for greater flexibility in choosing the system and options that suit each individual need:
Pressurization with CO2 Cartridges, bottled Nitrogen, or an in-house (user provided) source.
Single or double opening cells that accept different filter media.
Filter media that includes the API standard Filter Paper, Ceramic Discs of several calculated porosities, and various mesh sized screens.Ordering Information Part No. Cell Volts Watts 101565562 1800 psi Cell 115 800 101565564 1800 psi Cell 230 800 101565561 1800 psi Double Ended Cell 115 800 101565563 1800 psi Double Ended Cell 230 800 Specifications Rated working pressure 1800 PSIG Maximum temperature 500°F 115/230 VAC 50/60 Hz Sample Volume 493 ml Power Required 800 Watts
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Filter Press HPHT 175 ML
175 ml HPHT Filter Press units can be pressurized to 1800 psig on the cell and 750 psig on the back pressure receiver. Maximum operating temperature is 350°F.
HPHT Filter Presses are available in various component configurations to allow for greater flexibility in choosing the system and options that suit each individual need.
Pressurization with CO2 Cartridges, bottled Nitrogen, or an in-house (user provided) source.
Single or double opening cells that accept different filter media.
Filter media that includes the API standard Filter Paper, Ceramic Discs of several calculated porosities, and various mesh sized screens.Ordering Information Part No. Cell Description Volts Watts 101571372 1800 PSIG CO2 Pressurizing assembly
15 ml(CO2) Back-Pressure Receiver115 400 101571374 1800 PSIG CO2 Pressurizing assembly
15 ml (CO2) Back-Pressure Receiver230 400 101571373 1800 psi Double Ended Cell CO2 Pressurizing assembly
15 ml (CO2) Back-Pressure Receiver230 400 101565554 1800 psi Double Ended Cell Dual Nitrogen Manifold for Primary
15 ml Back Pressure Receiver115 400 101565558 1800 psi Double Ended Cell Dual Nitrogen Manifold for Primary
15 ml Back Pressure Receiver230 400 175 ml HPHT Filter Press units can be pressurized to 1800 psig on the cell and 750 psig on the back pressure receiver. Maximum operating temperature is 350°F. Specifications Rated working pressure 1800 PSIG Maximum temperature 350°F 115/230 VAC 50/60 Hz Sample Volume 173 ml Power Required 400 Watts Filtering Area 3.5 in2 Back Pressure Receiver Volume 15 ml
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Static Fluid Loss Test
Dual Cell Fluid Loss Test Assembly
The Fluid Loss Test Assembly provides a reliable means of determining the fluid loss characteristics of an oil well cement. Fluid Loss Testers measure fluid loss of cement slurries, drilling fluids, and fracturing fluids under elevated pressure and temperature conditions.
Fluid Loss Cells are fitted with a 325 mesh screen [3.5 in2 (22.6 cm2) filtration area] backed by a 60 mesh screen. The 60 mesh screen provides a flow path for the cement filtrate as outlined in API Recommended Practice 10B. Cells are provided with openings on both ends with caps (double ended) for ease of maintenance.Ordering Information Part No. Cells Volts 210195 Dual 115 210199 Dual 230 101502980 Single 115 101533370 Single 230 Specifications Rated working pressure 1,500 PSIG (10.35 MPa) Maximum temperature 200°F (93.33°C) Power Required 115/230 VAC 50/60 Hz Power Output 1,800 Watts Power Required 800 watts Filtering Area 3.5in2 (22.6 cm2)
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Stirring Fluid Loss Test
Conveniently located controls and indicators allow precise setting and control of temperature and pressure.
The Stirring Fluid Loss Test Assembly provides a reliable means of determining the fluid loss characteristics of an Oil Well Cement. This apparatus simulates down-hole conditions where fluid loss can occur. When cement slurry is circulated past a permeable zone, pressure behind the slurry can force fluid out of the slurry and into the zone. Circulation is simulated by a stirring apparatus and circulation temperature is simulated by a heating jacket. The pressure differential between annular and formation pressure is simulated by pressurized nitrogen. A screen (or porous core) and a filtration chamber simulate the permeable zone.
Slurry preconditioning and testing are performed in the same cell, eliminating the need to cool, or transfer hot test slurry, possibly changing the properties of the test slurry.
While the slurry is being heated, the stirring paddle maintains slurry uniformity. Nitrogen pressure is applied to the test fluid. Filtrate is forced through a filter medium. Fluid loss is measured as filtrate volume per unit of time.
Stirring Fluid Loss Cells are fitted with a 325 mesh screen [3.5 in² (22.6 cm²) filtration area] backed by a 60 mesh screen. The 60 mesh screen provides a flow path for the cement filtrate as outlined in API Recommended Practice 10B. Cells are provided with openings on both ends with caps (double ended) for ease of maintenance.Ordering Information Part No. Description 210194 Stirring Fluid Loss Assembly, 230 Volt, 50 Hz Specifications Rated working pressure 2,000 PSIG (13.8 MPa) Maximum temperature 400°F (204°C) Power Required 230 VAC, 9.0 Amps, 50/60 Hz Fluids Required Water for Cooling Pressurization Required Nitrogen Gas 1,500 psig (20 MPa) Filtering Area 3.5 in2 (22.6 cm2) Measured Properties Fluid Loss (ml/unit time)

